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New Akshully: NI-3 and IN-3, the black trigger 'scab' :-\ufffd
Makes the idea 'Debian Unstable' kinda laughable)(

Yup - that's the kind of stuff, alright..
Difference - my HS chem teach *Helped* !!

Sodium metal cut up into small chunks (under kerosene) - in bottle. In field. Rubber tube with funnel. Add water: watch white cloud slowly move across field.

No luck with the nitro (either). We at least realized that you either make very tiny qty (improbable) OR the whole hog + postage:

Fuming Sulfuric (Usual conc., but saturated with SO3). Hard to get and transport. Similar re the Nitroso- HNO3 - and Cooling Coils! to moderate the action. You just Can't get this (and the lore) together with any semblance of an excuse of saving lab, student + teacher-job.. y'know? (Which is why I hardly ever believe the "I made nitro" stories.)

And when I finally landed a summer+ job at Atlas Powder (not in Nitrating house) and first approached a loaded Angel Buggy .. an all-wood cart, squarish box (lined with ?), canvas hose with wooden pinch-cock: and realized fully the contained ENERGY, 'twas a Boom-geek's satori. Imagine *gallons* !!

Watching as the nitro was added to the mixer (for mere dynamite, Gelodyne IIRC) - through a plastic window. .. .. .. I could see it
SPLASHING !!!

over the powder already in the drum. Only the knowledge/faith? that this was routine.. routine.. routine..
kept the feets from sprint mode.

I attribute continued existence to:
A small tract some sharp (Insurance Co? - gotta see if I can find that) author assembled. Aptly titled, Challenge to Maturity it described some young .. alas-not-ept .. kiddies of similar bent, and a pipe bomb. Which exploded as the cap was screwed on. The carnage described delicately, incl. the relatively undamaged body of one miscreant - at the hospital. Until - -

they noted a red stain appearing on his side.. Bummer.

(I had never been reckless, in any case - but this did remind about overconfidence. Still, in the end, Luck is ever present. As with the phosgene generator. Or not. ;-)

Fulminates. Lead azide - Ah.. and I still have a couple pill bottles with various colorful yellow picrates, which time has proven to be - stable enough. What to do with the small sealed-in-glass bit of Rubidium metal? - and never forget the wondrous things you can do with a roll of thin Mg tape - either 'neat' or in combo. Entropy: there's the Thing.

{{cackle}} In the Lawyer Kultur - I suspect that our varied experiences shall be granted unto only a miniscule few of today's crop; maybe just as well - so many can't even add - let alone balance chem equations. What's in a MOL?


Ashton
Still regret letting someone have my Davis, [link|http://james-bond.cebru.com/books/P000gm8ggf9ngh/The_Chemistry_of_Powder_and_Explosives/| Chemistry of Powder and Explosives] :( in exchange for making a Ti part for my motorsickle.
New What, no chlorosulphonic acid?
Reacts with water to form both sulfuric and hydrochloric acids. [link|http://www.dmcc.com/chlorosulphonicacid1.html|Link].

IIRC, I used it in organic chemistry lab in high school to make some red dye.

And also in that Chem lab was [link|http://www.encyclopedia.com/html/p1/picricac.asp|picric acid], a nice yellow dye. Also known as 2,4,6-trinitrophenol, C6H2(NO2)3OH, and a cousin to trinitrotoluene (TNT). Yep, it's an explosive. Talk about a "dual use" material.

It's incredible now to think high school students had access to this stuff.
Alex

"Propaganda does not deceive people; it merely helps them to deceive themselves." -- Eric Hoffer
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         total geek but section2 question1 - (boxley) - (1)
             Just a geek, 20+. -NT - (a6l6e6x)
         Egads... I didn't think I was *that* bad... - (folkert)
         29.5858 - (drewk)
         The fact that I rushed to take this test - (tjsinclair)
         Unfair - (Andrew Grygus) - (7)
             Were you a chemistry geek? - (deSitter) - (6)
                 Re: Were you a chemistry geek? - (Andrew Grygus) - (5)
                     righteous! -NT - (deSitter)
                     Remember 'NI-3' - Iodine xtals + ammon. hydroxide? -NT - (Ashton) - (3)
                         Re: Remember 'NI-3' - Iodine xtals + ammon. hydroxide? - (Andrew Grygus) - (2)
                             Akshully: NI-3 and IN-3, the black trigger 'scab' :-\ufffd - (Ashton) - (1)
                                 What, no chlorosulphonic acid? - (a6l6e6x)
         Re: How geeky are YOU? - (Nightowl) - (5)
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                 Michi, of course. -NT - (admin)
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                 Note: - (admin)
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My pain became my strength I am reborn I'm deaf not dumb lest you forget.
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